Cytenamide acetic acid solvate
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چکیده
منابع مشابه
Cytenamide acetic acid solvate
IN THE CRYSTAL STRUCTURE OF THE TITLE COMPOUND (SYSTEMATIC NAME: 5H-dibenzo[a,d]cyclo-hepta-triene-5-carboxamide ethanoic acid solvate), C(16)H(13)NO·C(2)H(4)O(2), the cytenamide and solvent mol-ecules form a hydrogen-bonded R(2) (2)(8) dimer motif, which is further connected to form a centrosymmetric double ring motif arrangement. The cycloheptene ring adopts a boat conformation and the dihedr...
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Cytenamide forms a 1:1 solvate with trifluoro-acetic acid (systematic name: 5H-dibenzo[a,d]cyclo-hepta-triene-5-carboxamide trifluoro-acetic acid solvate), C(16)H(13)NO·C(2)HF(3)O(2). The compound crystallizes with one mol-ecule of cytenamide and one of trifluoro-acetic acid in the asymmetric unit; these are linked by O-H⋯O and N-H⋯O hydrogen bonds to form an R(2) (2)(8) motif. The trifluoro-me...
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Cytenamide forms a 1:1 solvate with butyric acid [systematic name: 5H-dibenzo[a,d]cyclo-hepta-triene-5-carboxamide-butanoic acid (1/1)], C(16)H(13)NO·C(4)H(8)O(2). The title compound crystallizes with one mol-ecule of cytenamide and one of butyric acid in the asymmetric unit; these mol-ecules are linked by N-H⋯O and O-H⋯O hydrogen bonds to form an R(2) (2)(8) heterodimer motif. Pairs of adjacen...
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IN THE CRYSTAL STRUCTURE OF THE TITLE COMPOUND [SYSTEMATIC NAME: 5H-dibenzo[a,d]cyclo-hepta-triene-5-carboxamide-meth-anoic acid (1/1)], C(16)H(13)NO·CH(2)O(2), the cytenamide and solvent mol-ecules form a hydrogen-bonded R(2) (2)(8) dimer motif, which is further connected to form a centrosymmetric double-motif arrangement. The asymmetric unit contains two formula units.
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In the title compound, C(20)H(18)N(4)·CH(3)COOH, the benzene ring forms dihedral angles of 81.34 (11) and 54.32 (11)° with the two pyridine rings. In the crystal, inter-molecular O-H⋯N hydrogen bonding links one 1,5-benzodiazepine mol-ecule and one acetic acid solvent mol-ecule into a dimer. These dimers, related by translation along the b axis, are further linked into chains via weak inter-mol...
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ژورنال
عنوان ژورنال: Acta Crystallographica Section E Structure Reports Online
سال: 2008
ISSN: 1600-5368
DOI: 10.1107/s160053680801550x